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Home > Publications > Electrochimie et Couches Minces

2014 - 2023

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1. 1. Gouget-Laemmel, A.-C.; Zidelmal, N.; Soares, R. S. B.; Barroca-Aubry, N.; Dragoe, D.; Costa, L.; Lepoittevin, B.; Salmi-Mani, H.; Mellah, M.; Henry-de-Villeneuve, C.; Ozanam, F.; Schulz, E.; Roger, P. Quantitative assessment of surface-initiated atom transfer radical polymerization brushes on silicon, ACS Applied Polymer Material,

2. Pacheco, I.; Bouvier, M.; Magnussen, O. M.; P. Allongue, P.; Maroun, F. Growth of ultrathin well-defined and crystalline films of Co3O4 and CoOOH by Electrodeposition, J. Electrochem. Soc. accepted,


1. 1. Bakangura, E.; Roger, P.; Soares, R. S. B.; Mellah, M.; Barroca-Aubry, N.; Gouget-Laemmel, A. C.; Ozanam, F.; Costa, L; Baltaze, J.-P.; Schulz, E. Post-modification of copolymers obtained by ATRP for an application in heterogeneous asymmetric salen catalysis. Molecules, 27 (2022), 4654,

2. Colon-Quintana, G. S.; Vannoy, K. J.; Renault, C.; Voci, S.; Dick, J. E. Tuning the Three-Phase Microenvironment Geometry Promotes Phase Formation, Journal of Physical Chemistry C, 126 (2022) 20004-20010,

3. Feng, Y.; Cheriet, A.; Panagopoulou, M.; Henry-de-Villeneuve, C.; Rosso, M.; Ozanam, F. Controlling homogeneity of the first lithiation in methylated amorphous silicon, Electrochimica Acta 403 (2022) 139655,

4. Feng, Y.; Koo, B. M.; Seyeux , A.; Światowska, J.; Henry-de-Villeneuve, C.; Rosso, M.; Ozanam, F. ToF-SIMS Li depth profiling of pure and methylated amorphous silicon electrodes after their partial lithiation, ACS Appl. Mater. Interfaces 14 (2022) 35716-35725,

5. Kazan, R.; Bourgeois, G.; Carisetti, D.; Florea, I.; Larquet, E.; Maurice, J.-L.; Mechulam, Y.; Ozanam, F.; Schmitt, E.; Coureux, P.-D. Grid batch-dependent tuning of glow discharge parameters, Front. Mol. Biosci., 9 (2022) 910218,

6. Nuy, T. P.; Kilinc, V.; Hayakawa, R.; Henry-de-Villeneuve, C.; Raimundo, J.-M.; Wakayama, Y.; Charrier, A. Affinity driven ion exchange EG-OFET sensor for high selectivity and low limit of detection of Cesium in seawater, Sensors & Actuators B: Chemical 351 (2022) 130956,

7. Renault, C.; Laborde, C.; Cossettini, A.; Selmi, L.; Widdershoven, F.; Lemay, S. G. Electrochemical characterization of individual oil micro-droplets by high-frequency nanocapacitor array imaging, Faraday Discussions, 233 (2022) 175-189,

8. Wiegmann, T.; Pacheco, I.; Reikowski, F.; Stettner, J.; Qiu, C.; Bouvier, M.; Bertram, M.; Faisal, F.; Brummel, O.; Libuda, J.; Drnec, J.; Philippe Allongue, P.; Maroun, F.; Magnussen, O. M. Operando identification of the reversible skin layer on Co3O4 as a three-dimensional reaction zone for oxygen evolution, ACS Catal. 12 (2022) 3256–3268,

9. Yuan, H.; Fu, W.; Soulmi, N.; Serre, C.; Steunou, N.; Rosso, M.; Henry-de-Villeneuve, C. Growth of Fe-BDC Metal Organic Frameworks onto functionalized Si (111) surfaces, Chemistry - An Asian Journal 17 (2022) e202200129,


1. Andrei, C.-C.; Moraillon, A.; Larquet, E.; Potara, M.; Astilean, S.; Jakab, E.; Bouckaert, J.; Rosselle, L.; Skandrani, N.; Boukherroub, R.; Ozanam, F.; Szunerits, S.; Gouget-Laemmel, A. C. SERS characterization of aggregated and isolated bacteria deposited on silver-based substrates. Analytical and Bioanalytical Chemistry, 413 (2021), 1417-1428,

2. Deng, Z. J.; Renault, C. Detection of individual insulating entities by electrochemical blocking,
Current Opinion in Electrochemistry 25 (2021) 100619,

3. Deng, Z. J.; Renault, C. Unravelling the last milliseconds of an individual graphene nanoplatelet before impact with a Pt surface by bipolar electrochemistry, Chemical Science 12 (2021) 12494-12500,

4. Fournier, O.; Darin Bapaume, C.; Messou, D.; Bouttemy, M.; Schulz, P.; Ozanam, F; Lombez, L.; Schneider, N.; Rousset, J. Chemical Passivation with Phosphonic Acid Derivatives of ZnO Deposited by Atomic Layer Deposition and Its Influence on the Halide Perovskite Interface, ACS Appl. Energy Mater., 4 (2021) 5787-5797,

5. Miki, A.; Nishikawa, K.; Kamesui, G.; Matsushima, H.; Ueda, M.; Rosso, M. In-situ Interferometry Study of ionic mass transfer phenomenon during the electrodeposition and dissolution of Li metal in solvate ionic liquids, J. Mater. Chem. A 9 (2021) 14700-14709,

6. Pendergast, A. D.; Deng, Z. J.; Maroun, F.: Renault, C; Dick, J. E. Revealing Dynamic Rotation of Single Graphene Nanoplatelets on Electrified Microinterfaces, ACS Nano 15 (2021) 1250-1258,

7. Pendergast, A. D.; Renault, C; Dick, J. E. Correlated Optical-Electrochemical Measurements Reveal Bidirectional Current Steps for Graphene Nanoplatelet Collisions at Ultramicroelectrodes, Analytical Chemistry 93 (2021) 2898-2906,


1. 1. Andrei, C.-C.; Moraillon, A.; Lau, S. ; Felidj, N.; Yamakawa, N.; Bouckaert, J.; Larquet, E.; Boukherroub, R.; Ozanam, F.; Szunerits, S.; Gouget-Laemmel, A. C. Rapid and sensitive identification of uropathogenic Escherichia coli using a surface-enhanced-Raman-scattering-based biochip Surface Enhanced Raman Spectroscopy (SERS), Talanta, 219 (2020) 121174,

2. Aschl, T.; Frison, G.; Moraillon, A.; Ozanam, F.; Allongue, P.; Gouget-Laemmel, A. C. Insights into the ochratoxin A / aptamer interactions on silicon by UV-Vis & FTIR studies. Langmuir, 36 (2020), 13908-13917,

3. Deng, Z. J.; Maroun, F; Dick, J. E.; Renault, C. Detection of individual conducting graphene nanoplatelet by electro-catalytic depression, Electrochimica Acta 355 (2020) 136805,

4. Grumelli, D.; Wiegmann, T.; Barja, S.; Reikowski, F.; Maroun, F.; Allongue, P.; Balajka, J.; Parkinson, G. S.; Diebold, U.; Kern, K.; Magnussen, O. M. Electrochemical stability of the reconstructed Fe3O4(001) surface, Angewandte Chemie Int. Ed., 59 (2020) 1-6, and

5. Moazzenzade, T.; Yang, X.J.; Walterbos, L.; Huskens, J.; Renault, C.; Lemay, S. G. Self-Induced Convection at Microelectrodes via Electroosmosis and Its Influence on Impact Electrochemistry, Journal of the American Chemical Society, 142 (2020) 17908-17912,

6. Renault, C.; Lemay, S. G. Electrochemical Collisions of Individual Graphene Oxide Sheets: An Analytical and Fundamental Study, ChemElectroChem, 7 (2020) 69-73,

7. Wiegmann, T.; Drnec, J.; Reikowski, F.; Stettner J.; Maroun F.; Magnussen, O. M. In Situ Transmission X-ray Micro-Diffraction from Thin Metal Films Electrodeposited in Microfluidic Channels, J. Electrochem. Soc. 167 (2020) 112505,


1. 1. Bongu, C; Surble, S.; Alper, Dr. J.; Boulineau, A.; Martin, J.-F.; Demarque, A.; Coulon, P.-E.; Rosso, M.; Ozanam, F.; Franger, S.; Herlin-Boime, N.; Le Caer, S. Artificial Solid Electrolyte Interphase Formation on Si Nanoparticles through Radiolysis: Importance of the Presence of an Additive, J. Phys. Chem. C 123 (2019) 28550-28560,

2. Feng, Y.; Ngo, T.-D.-T.; Panagopoulou, M.; Cheriet, A.; Koo, B.M.; Henry-de-Villeneuve, C.; Rosso, M.; Ozanam, F. Lithiation of pure and methylated amorphous silicon: monitoring by operando optical microscopy and ex situ atomic force microscopy Electrochim. Acta 302 (2019) 249-258,

3. Glasscott, M. W.; Pendergast, A. D.; Goines, S.; Bishop, A. R.; Hoang, A. T.; Renault, C.; Dick, J. E. Electrosynthesis of high-entropy metallic glass nanoparticles for designer, multi-functional electrocatalysis, Nature Communications, 10 (2019) 2650,

4. Henry de Villeneuve, C.; Nguyen-Le, T. L.; Ozanam, F.; Allongue P. Structure of Mixed Acid/Decyl Monolayers Grafted on Oxide-Free Si(111) Surfaces, Langmuir, 35 (2019) 2547-2553,

5. Kilinc, V.; Henry-de-Villeneuve, C.; Nguy, T. P.; Wakayama, Y.; Charrier, A.; Raimundo, J.-M. Novel and innovative interface as potential active layer in Chem-FET sensor devices for the specific sensing of Cs2+, ACS Applied Materials & Interfaces 11 (2019) 47635-47641,

6. Klaes, S.; Henry de Villeneuve, C.; Ozanam, F .; Barta, C.; Rück-Braun, K.; Métivier, R.; Allongue, P. Influence of Light Polarization on Photoswitching of Fulgimide Monolayers on Surfaces, J. Phys. Chem. C, 123 (2019) 12223-12233,

7. Lamirand, A. D.; Adam, J.-P.; Ravelosona, D.; Allongue, P.; Maroun, F. In Situ Monitoring of Electric Field Effect on Domain Wall Motion in Co Ultrathin Films in Direct Contact with an Electrolyte, Appl. Phys. Lett., 2019, 115, 032402,

8. Pendergast, A. D.; Glasscott, M. W.; Renault, C.; Dick, J. E. One-step electrodeposition of ligand-free PdPt alloy nanoparticles from water droplets: Controlling size, coverage, and elemental stoichiometry, Electrochemistry Communications 98 (2019) 1-5,

9. Reikowski, F.; Maroun F.; Pacheco, I.; Wiegmann, T.; Allongue, P.; Stettner, J.; Magnussen, O. M. Operando Surface X-ray Diffraction Studies of Structurally-defined Co3O4 and CoOOH Thin Films during Oxygen Evolution, ACS Catalysis, 9 (2019) 3811-3821,

10. Wakerley, D.; Lamaison, S.; Ozanam, F.; Menguy, N.; Mercier, D.; Marcus, P.; Fontecave, M.; Mougel, V. Bio-inspired hydrophobicity promotes CO2 reduction on a Cu surface, Nature Materials, 18 (2019) 1222-1227,


[1] Penafiel-Castro, J. A.; Hahn, B.; Maltez, R. L.; Knornschild, G.; Allongue, P.; Dick, L. F. P. Direct Li+ incorporation during the anodic formation of compact TiO2 layers, Chemical Communications, 54 (2018) 3251, DOI 10.1039/c8cc00829a

[2] Zidelmal, N.; Aubry-Barroca, N.; Lepoittevin, B.; Mellah, M.; Costa, L.; Ozanam, F.; Gouget-Laemmel, A. C.; Schulz, E.; Roger, P. Synthesis, characterization and catalytic properties of salen-containing polymers obtained by atom transfer radical polymerization, Polymer, 135 (2018) 261, DOI 10.1016/j.polymer.2017.12.019

[3] Hahn, W.; Lentali, J. M.; Polovodov, P.; Young, N.; Nakamura, S.; Speck, J. S.; Weisbuch, C.; Filoche, M.; Wu, Y. R.; Piccardo, M.; Maroun, F.; Martinelli, L.; Lassailly, Y.; Peretti, J. Evidence of nanoscale Anderson localization induced by intrinsic compositional disorder in InGaN/GaN quantum wells by scanning tunneling luminescence spectroscopy, Physical Review B, 98 (2018), DOI

[4] Brunet, M.; Aureau, D.; Guillemot, F.; Etcheberry, A.; Ozanam, F.; Gouget-Laemmel, A. C. The critical role of wavelength in the UV-activated grafting of 1-alkene onto silicon and silicon nitride SixN4 surfaces, Chemical Communications, 54 (2018) 7167, DOI

[5] Maroun, F.; Reikowski, F.; Di, N.; Wiegmann, T.; Stettner, J.; Magnussen, O. M.; Allongue, P. Potential dependence of the structure and magnetism of electrodeposited Pd/Co/Au(111) layers, Journal of Electroanalytical Chemistry, 819 (2018) 322, DOI

[6] Koo, B. M.; Dalla Corte, D. A.; Chazalviel, J. N.; Maroun, F.; Rosso, M.; Ozanam, F. Lithiation Mechanism of Methylated Amorphous Silicon Unveiled by Operando ATR-FTIR Spectroscopy, Advanced Energy Materials, 8 (2018) 1702568, DOI: 10.1002/aenm.201702568


Transmission Surface Diffraction for Operando Studies of Heterogeneous Interfaces
F Reikowski, T Wiegmann, J Stettner, J Drnec, V Honkimaki, F Maroun, P Allongue, and O M Magnussen
Journal of Physical Chemistry Letters 8 (2017) 1067.

Etching and Chemical Control of the Silicon Nitride Surface
M Brunet, D Aureau, P Chantraine, F Guillemot, A Etcheberry, A C Gouget-Laemmel, and F Ozanam
Acs Applied Materials & Interfaces 9 (2017) 3075.


[1] Ozanam, F.; Rosso, M. Silicon as anode material for Li-ion batteries, Materials Science and Engineering B-Advanced Functional Solid-State Materials, 213 (2016) 2, DOI 10.1016/j.mseb.2016.04.016

[2] Kim, J.; Renault, C.; Nioradze, N.; Arroyo-Curras, N.; Leonard, K. C.; Bard, A. J. Nanometer Scale Scanning Electrochemical Microscopy Instrumentation, Analytical Chemistry, 88 (2016) 10284, DOI 10.1021/acs.analchem.6b03024

[3] Allongue, P.; Magnussen, O. Foreword, Electrochimica Acta, 213 (2016) 270, DOI 10.1016/j.electacta.2016.07.031

[4] Jurca, H. F.; Damian, A.; Gougaud, C.; Thiaudiere, D.; Cortes, R.; Maroun, F.; Allongue, P. Epitaxial Electrodeposition of Fe on Au(111): Structure, Nucleation, and Growth Mechanisms, Journal of Physical Chemistry C, 120 (2016) 16080, DOI 10.1021/acs.jpcc.5b12771

[5] Kim, J.; Renault, C.; Nioradze, N.; Arroyo-Curras, N.; Leonard, K. C.; Bard, A. J. Electrocatalytic Activity of Individual Pt Nanoparticles Studied by Nanoscale Scanning Electrochemical Microscopy, Journal of the American Chemical Society, 138 (2016) 8560, DOI 10.1021/jacs.6b03980

[6] Dalla Corte, D. A.; Gouget-Laemme, A. C.; Lahlil, K.; Caillon, G.; Jordy, C.; Chazalviel, J. N.; Gacoin, T.; Rosso, M.; Ozanam, F. Molecular grafting on silicon anodes: artificial Solid-Electrolyte Interphase and surface stabilization, Electrochimica Acta, 201 (2016) 70, DOI 10.1016/j.electacta.2016.03.105

[7] Lecadre, F.; Maroun, F.; Allongue, P. Electrodeposition of Ag, Pd and Au on Ni monolayer islands on (1 x 1)-Au(111) by in-situ scanning tunneling microscopy, Electrochimica Acta, 197 (2016) 241, DOI 10.1016/j.electacta.2016.02.124
[8] Reikowski, F.; Maroun, F.; Di, N.; Allongue, P.; Ruge, M.; Stettner, J.; Magnussen, O. M. In situ surface X-ray diffraction study of ultrathin epitaxial Co films on Au(111) in alkaline solution, Electrochimica Acta, 197 (2016) 273, DOI 10.1016/j.electacta.2016.01.052

[9] Lucas, C. A.; Maroun, F.; Sisson, N.; Thompson, P.; Grunder, Y.; Cortes, R.; Allongue, P. Film and Interface Atomic Structures of Electrodeposited Co/Au(111) Layers: An in Situ X-ray Scattering Study as a Function of the Surface Chemistry and the Electrochemical Potential, Journal of Physical Chemistry C, 120 (2016) 3360, DOI 10.1021/acs.jpcc.5b11107

[10] Yang, J.; Siriwardena, A.; Boukherroub, R.; Ozanam, F.; Szunerits, S.; Gouget-Laemmel, A. C. A quantitative method to discriminate between non-specific and specific lectin-glycan interactions on silicon-modified surfaces, Journal of Colloid and Interface Science, 464 (2016) 198, DOI 10.1016/j.jcis.2015.11.018

[11] Philipsen, H. G. G.; Ozanam, F.; Allongue, P.; Kelly, J. J.; Chazalviel, J. N. In-situ infrared study of silicon in KOH electrolyte: Surface hydrogenation and hydrogen penetration, Surface Science, 644 (2016) 180, DOI 10.1016/j.susc.2015.10.040

[12] Di, N.; Damian, A.; Maroun, F.; Allongue, P. Influence of Potential on the Electrodeposition of Co on Au(111) by In Situ STM and Reflectivity Measurements, Journal of the Electrochemical Society, 163 (2016) D3062, DOI 10.1149/2.0091612jes

[13] Damian, A.; Maroun, F.; Allongue, P. Electrochemical de-alloying in two dimensions: role of the local atomic environment, Nanoscale, 8 (2016) 13985, DOI 10.1039/c6nr01390b

[14] Philipsen, H. G. G.; Ozanam, F.; Allongue, P.; Kelly, J. J.; Chazalviel, J. N. Oxide Formation and Dissolution on Silicon in KOH Electrolyte: An In-Situ Infrared Study, Journal of the Electrochemical Society, 163 (2016) H327, DOI 10.1149/2.0911605jes

[15] Dalla Corte, D. A.; Caillon, G.; Jordy, C.; Chazalviel, J. N.; Rosso, M.; Ozanam, F. Spectroscopic Insight into Li-Ion Batteries during Operation: An Alternative Infrared Approach, Advanced Energy Materials, 6 (2016) 1501768, DOI 10.1002/aenm.201501768


[1] Khaldi, K.; Sam, S.; Gouget-Laemmel, A. C.; de Villeneuve, C. H.; Moraillon, A.; Ozanam, F.; Yang, J.; Kermad, A.; Ghellai, N.; Gabouze, N. Active Acetylcholinesterase Immobilization on a Functionalized Silicon Surface, Langmuir, 31 (2015) 8421, DOI 10.1021/acs.langmuir.5b01928

[2] Yang, J.; Moraillon, A.; Siriwardena, A.; Boukherroub, R.; Ozanam, F.; Gouget-Laemmel, A. C.; Szunerits, S. Carbohydrate Microarray for the Detection of Glycan-Protein Interactions Using Metal-Enhanced Fluorescence, Analytical Chemistry, 87 (2015) 3721, DOI 10.1021/ac504262b

[3] Di, N.; Kubal, J.; Zeng, Z.; Greeley, J.; Maroun, F.; Allongue, P. Influence of controlled surface oxidation on the magnetic anisotropy of Co ultrathin films, Applied Physics Letters, 106 (2015) 122405, DOI 10.1063/1.4916554

[4] Kaiber, A.; Cherkaoui, M.; Chazalviel, J. N.; Ozanam, F. Reactivity Study of Silicon Electrode Modified by Grafting Using Electrochemical Reduction of Diazonium Salts, Journal of the Chemical Society of Pakistan, 37 (2015) 68, DOI

[5] Tournerie, N.; Engelhardt, A.; Maroun, F.; Allongue, P. Probing the electrochemical interface with in situ magnetic characterizations: A case study of Co/Au(111) layers, Surface Science, 631 (2015) 88, DOI 10.1016/j.susc.2014.06.023

[6] Lecadre, F.; Damian, A.; Braems, I.; Maroun, F.; Allongue, P. Ni electrochemical epitaxy on unreconstructed Au(111): An in-situ STM study, Surface Science, 631 (2015) 135, DOI 10.1016/j.susc.2014.06.014

[7] Kaiber, A.; Amiar, A.; Cherkaoui, M.; Chazalviel, J. N.; Ozanam, F. Study of grafting on silicon by electrochemical reduction of methoxybenzene diazonium, Annales De Chimie-Science Des Materiaux, 39 (2015) 41, DOI 10.3166/acsm.39.41-51


[1] Slimani, A.; Iratni, A.; Henry, H.; Plapp, M.; Chazalviel, J. N.; Ozanam, F.; Gabouze, N. Macropore formation in p-type silicon: toward the modeling of morphology, Nanoscale Research Letters, 9 (2014) 585, DOI 10.1186/1556-276x-9-585

[2] Yang, J.; Chazalviel, J. N.; Siriwardena, A.; Boukherroub, R.; Ozanam, F.; Szunerits, S.; Gouget-Laemmel, A. C. Quantitative Assessment of the Multivalent Protein-Carbohydrate Interactions on Silicon, Analytical Chemistry, 86 (2014) 10340, DOI 10.1021/ac502624m

[3] Pereira-Nabais, C.; Swiatowska, J.; Rosso, M.; Ozanam, F.; Seyeux, A.; Gohier, A.; Tran-Van, P.; Cassir, M.; Marcus, P. Effect of Lithiation Potential and Cycling on Chemical and Morphological Evolution of Si Thin Film Electrode Studied by ToF-SIMS, Acs Applied Materials & Interfaces, 6 (2014) 13023, DOI 10.1021/am502913q

[4] Presle, M.; Maurin, I.; Maroun, F.; Cortes, R.; Lu, L. L.; Hassan, R. S.; Larquet, E.; Guigner, J. M.; Riviere, E.; Wright, J. P.; Boilot, J. P.; Gacoin, T. Photostrictive/Piezomagnetic Core-Shell Particles Based on Prussian Blue Analogues: Evidence for Confinement Effects?, Journal of Physical Chemistry C, 118 (2014) 13186, DOI 10.1021/jp501758b

[5] Carugno, S.; Chassaing, E.; Rosso, M.; Gonzalez, G. A. Enhanced electrochemical oxidation of methanol on copper electrodes modified by electrocorrosion and electrodeposition, Materials Chemistry and Physics, 143 (2014) 1012, DOI 10.1016/j.matchemphys.2013.10.039

[6] Sam, S.; Gouget-Laemmel, A. C.; Chazalviel, J. N.; Ozanam, F.; Etcheberry, A.; Belhousse, S.; Gabouze, N. Voltammetric behavior of peptide-modified porous silicon after metal complexation. In Materials and Applications for Sensors and Transducers Iii; Hristoforou, E., Vlachos, D. S., Eds., 2014; Vol. 605; pp 119, DOI 10.4028/

[7] Souza, A. L.; Tremiliosi-Filho, G.; Kubota, L. T.; Mendes, R. K.; do Rego, A. M. B.; Oliveira, O. N.; de Villeneuve, C. H.; Chazalviel, J. N.; Allongue, P.; Ozanam, F.; Rodrigues, U. P. Poly(dimethylsiloxane) as a pre-coating in layer-by-layer films containing phosphotungstate nanoclusters electrochemically sensitive toward s-triazines, Rsc Advances, 4 (2014) 29612, DOI 10.1039/c4ra01468e